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AKTU Modern Analytical Techniques (Practical) (BP709P) Syllabus PDF – B.Pharm 7th Semester
Modern Analytical Techniques (Practical) BP709P
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Official AKTU syllabus of Modern Analytical Techniques (Practical) (BP709P) for B.Pharm 7th Semester – 1 credits, L-T-P 0-0-3. Read the unit-wise course content, course outcomes, evaluation pattern and recommended books online, or download the PDF.
Syllabus — Modern Analytical Techniques (Practical)
Download PDFBP709P · 1 credits · L-T-P 0-0-3
Course Objectives
- Provide practical training in interpretation of advanced instrumental data used for structural and physicochemical characterization.
- Introduce quantitative analytical techniques using modern separation methods, such as UHPLC and HPLC, for the estimation of pharmaceutical substances.
- Familiarize students with the principles and practice of green analytical chemistry, including preparation of green solvents and development of environmentally sustainable analytical methods.
- Develop understanding of bioanalytical sample preparation techniques for pharmaceutical analysis in biological matrices, including solid phase extraction, liquid liquid extraction, and protein precipitation.
- Learn applied pharmaceutical analysis and methods including cell viability assays, residual solvent analysis, and estimation of drugs from biological fluids.
Course Outcomes
| CO | Upon successful completion of this course, the students will be able to: |
| No. | |
| 1 | Analyze and interpret proton NMR, carbon NMR, mass spectra, X-Ray diffraction patterns, and DSC thermograms to characterize pharmaceutical compounds. |
| 2 | Perform quantitative analysis of official pharmaceutical compounds using UHPLC. |
| 3 | Design and assess the suitability of green analytical solvents for pharmaceutical applications, promoting sustainability. |
| 4 | Construct a comprehensive protocol for bioavailability and bioequivalence studies adhering to USFDA regulatory standards. |
| 5 | Employ appropriate extraction techniques (SPE, PPE, LLE) for the accurate quantification of pharmaceuticals in biological fluids and matrices and explain and execute the MTT assay for evaluating cell viability in a laboratory setting. |
Course Content
List of Practicals (Minimum 12 experiments must be performed)
- Interpretation of Proton NMR spectra of known compound (any two)
- Interpretation of Carbon NMR spectra of known compound (any two)
- Interpretation of mass spectrum of known compound (any two)
- Interpretation of X-Ray diffraction spectrum (any one)
- Interpretation of DSC Thermogram (any one)
- Preparation and Evaluation of Green Analytical Solvents
- Analytical method development by using Green chemistry
- Quantification of pharmaceuticals in biological fluids using Solid Phase Extraction (SPE)
- Quantification of pharmaceuticals in biological matrix by PPE
- Quantification of pharmaceuticals in biological matrix by LLE
- Demonstration of Cell Viability evaluation using MTT Assay
- Demonstration on residual solvent analysis using GC
- Assay of drug using HPLC (any two)
- Analysis of drug from biological fluid using HPLC/ UV spectroscopy.
Recommended References
- Beckett, A. H. and Stenlake, J. B. Practical Pharmaceutical Chemistry. CBS Publishers & Distributors.
- Brittain, H. G. Analytical Profiles of Drug Substances and Excipients. Elsevier.
- Kemp, W. Organic Spectroscopy. Palgrave Macmillan.
- Munson, J. W. Pharmaceutical Analysis: Modern Methods. Marcel Dekker.
- Sethi, P. D. Quantitative Analysis of Drugs in Pharmaceutical Formulations. CBS Publishers & Distributors.
- Sharma, B. K. Instrumental Methods of Chemical Analysis. Goel Publishing House.
- Sharma, Y. R. Organic Spectroscopy. S. Chand.
- Silverstein, R. M., Webster, F. X., Kiemle, D. J. and Bryce, D. L. Spectrometric Identification of Organic Compounds. Wiley.
- Willard, H. H., Merritt, L. L., Dean, J. A. and Settle, F. A. Instrumental Methods of Analysis. Brooks/Cole.
- Indian Pharmacopoeia. Indian Pharmacopoeia Commission.
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