AKTU Analysis and Characterization of Polymers (BPE061) Syllabus PDF – B.Tech 3rd Year
Analysis and Characterization of Polymers BPE061
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- Semester 6
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Syllabus — Analysis and Characterization of Polymers
Download PDFBPE061 · 3 credits · L-T-P 3-0-0
Course Outcomes
| Course Outcomes: The students will be able to | Blooms Taxonomy | |
| CO‐1 | Have knowledge about various aspects of X‐ray diffractometry | K2 |
| CO‐2 | Attain knowledge about various types of microscopy | K2 |
| CO‐3 | Have understanding of various spectroscopic methods | K2 |
| CO‐4 | Analyze various methods of molecular characterization of polymers | K3 |
| CO‐5 | Analyze the data taken by thermal characterization of polymers | K3 |
Molecular Characterization of Polymers Determination of molecular weight, viscometry, end group analysis, colligative property, osmometry, light scattering technique, determination of molecular weight and molecular weight distribution, gel permeation chromatography (GPC).
Thermal Analysis Techniques Differential thermal analysis (DTA), differential scanning calorimetry (DSC), thermogravimetric analysis (TGA), thermomechanical analysis (TMA), dynamic mechanical thermal analysis (DMTA).
X‐ray diffractometry X‐ray diffraction analysis, experimental methods, applications‐Chain conformations, chain packing, disorder in the crystal, degree of Crystallinity, micro structural parameters, degree of orientations.
Principles of microscopy Optical, SEM, TEM, AFM; Morphology of polymers, Crystallization behavior, phase separation and applications UV/Visible Spectroscopy Introduction, principle, Lambert law, Beer’s law, theory, instrumentation, procedure, advantages, disadvantages, interpretation of spectrogram, applications‐qualitative analysis, quantitative analysis; purity, cis‐ and trans‐ conformation.
Fourier transform infrared (FTIR) spectroscopy, Introduction, principle, theory, instrumentation, ATR attachment, methods of sample preparation, advantages, disadvantages, interpretation of spectra, applications, establishment of chemical structure of polymers, reaction kinetics, polymer linkage, hydrogen bond formation, purity, copolymerization, qualitative and quantitative results, gas chromatograph (GC) ‐ Mass spectrometer.
Nuclear Magnetic Resonance(NMR) spectroscopy, (1H NMR and 13C NMR), Introduction, Principle, theory, Spin‐spin coupling, coupling constant – chemical shifts ‐ instrumentation, procedure, method of sample preparation ‐ applications – chemical structures, purity, tacticity, Solid state NMR – applications.
Text Books :‐
- Nicholas P. Cheremisinoff, Polymer characterization – Laboratory Techniques and Analysis, Elsevier Books.
- Hunt & James, Polymer characterization – Chapman & Hall, London, 1993 References :‐
- ASTM – Volume: 8.01, 8.02 & 8.03, 2000
- G. Kämpf, Characterization of plastics using physical methods, Experimental techniques and practical applications. Hanser Publishers, Munich, 1986
- D. Campbell & J.R. White, Polymer Characterization, Chapman & Hall, 1989.
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